BEAMLINE GUIDE
APS 22-ID (SER-CAT)
The Advanced Photon Source
Argonne, IL
ALS Automounter
22ID is a protein crystallographic beamline. It has an ALS style sample changer with a capacity of 230 samples. Its primary detector is a Eiger 16M detector.
Supported Techniques
- Macromolecular crystallography
- Multi-wavelength anomalous dispersion
- Single-wavelength anomalous dispersion
- Microbeam
Beamline Controls and Data Acquisition
Beamline control and data acquisition software: MX system. DC-servomotor; PMAC motor controller electrometer amplifiers; VME-based, computer controlled V/F converter and scaler (ANL-ECT design).
Detectors
- Eiger 16M
Additional Equipment
- MD2 micro diffractometer
- 225 sample ALS style robot
- Liquid nitrogen cryosystem sample cooler
- Sample mounting microscopes
- Equipped chemical laboratory 1
Contacts
John Chrzas
Lily Li
Norma Duke
Other Links
Tools
We recommend the following tools for their compatibility and ease-of-use.
Recommended | Accepted* | |
---|---|---|
Puck Style | Uni-Puck | Uni-Puck, ALS |
Mount/Loop Style | MicroMounts™ & MicroLoops™ LD | Any |
Rod Length | 18mm | 18mm |
Base Style | B1A-Reusable | B1A-Reusable, B1A, B3S-Reusable, B3S |
*The SER-CAT Spectrum. p 6. Retrieved November 4, 2013. |
Sample Preparation Kits
Convenient kits of compatible assemblies of MiTeGen recommended products
Beamline Sample Preparation Kits are available in 3 aperture size assortments based on your crystal sizes and include:
- Assemblies of 100 Crystal Mounts, on 18 mm pins, available in the following assortment:
- 20 x Dual-Thickness MicroLoops ™ LD (5 each of 10, 20, 30 and 50 μm aperture sizes)
- 40 x Dual-Thickness MicroMount ™ (10 each of 75, 100, 150 and 200 μm aperture sizes)
- 20 x Dual-Thickness MicroLoops ™ (5 each of 300, 400, 500 and 600 μm aperture sizes)
- 20 x MicroMeshes ™ (5 each of 10, 25, 50 and 25L μm aperture sizes)
- Installed in 100 B5-R reusable bases or 100 regular bases
- Packaged and stored in 5 MiTeGen base holders
Uni-puck Starter Kit 2 includes:
- (7) Universal V-1 Pucks
- (1) Double Puck Loading Dewar with Lid
- (1) Puck Wand
- (1) Puck Dewar Loading Tool
- (1) Puck Separator Tools
- (1) Shelved Puck Shipping Cane
- (1) Bent Cryo-Tong
- (1) Cryo Express Dry Shipper (CX100)
- (1) Shipping case for CX100
*custom kits are available, contact MiTeGen with specific requests.
Order Beamline Kits
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Small Aperture Assortment Beamline Sample Preparation Kit
100 Dual Thickness MicroMounts™ (25 each of 10, 20, 30 and 50 μm aperture DT MicroMounts™) On standard... -
Medium Aperture Assortment Beamline Sample Preparation Kit
100 Dual Thickness MicroMounts™ (25 each of 75, 100, 150 and 200 μm aperture DT MicroLoops™) On standard... -
Large Aperture Assortment Beamline Sample Preparation Kit
100 Dual Thickness MicroLoops™ (25 each of 300, 400, 500 and 600 μm aperture DT MicroLoops™) On standard... -
Universal Puck (Uni-Puck) Starter Kits
To get you up–and–running sending samples to the beamline in easy-to-order bundles. Full Description