BEAMLINE GUIDE
SPring–8 BL44B2


Super Photon ring-8 GeV
Japan
SPACE Automounter

The BL44B2 is a materials science beamline using high-energy powder diffractometry. The main scientific purpose is to reveal correlations between structures and properties in novel functional materials based on the charge density structure. To achieve the purpose, the optical parameters have been optimized and the powder diffractometer has been developed. Taking advantage of the beamline, high counting statistics and high angular resolution data can be collected in several minutes from powder samples with several milligrams. The white beam generated from the SPring-8 standard bending magnet is monochromatized and focused by the optical components. The beam optimized for powder samples sealed in a glass capillary is irradiated to the samples on the diffractometer, by which a camera method with transmission geometry allows to collect a whole diffraction pattern simultaneously.1

Automated Systems at BL44B2:

“To achieve high-throughput protein crystallography, we have developed two special components: an automated sample changer robot, SPACE (SPring-8 precise auto-matic cryo-sample exchanger) (Ueno, Hirose et al., 2004), which can change up to 100 crystals in a diffractometer, and the beamline control software BSS (beamline scheduling software) (Ueno et al., 2005), which can perform successive data collection by controlling beamline devices, including SPACE, and managing the data collection schedule. The combination of SPACE and BSS enables unmanned overnight data collection and allows the beamline to operate with high efficiency.” 2


Contacts


Tools

We recommend the following tools for their compatibility and ease-of-use.

Recommended Accepted*
Puck Style Uni-PuckALSACTORSPACE tray
Mount/Loop Style Any
Rod Length 18mm/SPINE
Base Style B1A-Reusable, B1-RB3-RB3S-RB5-RSPACE pin
*Robotic Sample Handling, Aina Cohen. Retrieved December 9, 2013.

To purchase ACTOR pucks, please contact us.


Sample Preparation Kits

Convenient kits of compatible assemblies of MiTeGen recommended products

Beamline Sample Preparation Kits are available in 3 aperture size assortments based on your crystal sizes and include:

  • Assemblies of 100 Crystal Mounts, on 18 mm pins, available in the following assortment:
    • 20 x Dual-Thickness MicroLoops ™ LD  (5 each of 10, 20, 30 and 50 μm aperture sizes)
    • 40 x Dual-Thickness MicroMount ™ (10 each of 75, 100, 150 and 200 μm aperture sizes)
    • 20 x Dual-Thickness MicroLoops ™  (5 each of 300, 400, 500 and 600 μm aperture sizes)
    • 20 x MicroMeshes ™  (5 each of 10, 25, 50 and 25L μm aperture sizes)
  • Installed in 100 B5-R reusable bases or 100 regular bases
  • Packaged and stored in 5 MiTeGen base holders

Uni-puck Starter Kit 2 includes:

  • (7) Universal V-1 Pucks
  • (1) Double Puck Loading Dewar with Lid
  • (1) Puck Wand
  • (1) Puck Dewar Loading Tool
  • (1) Puck Separator Tools
  • (1) Shelved Puck Shipping Cane
  • (1) Bent Cryo-Tong
  • (1) Cryo Express Dry Shipper (CX100)
  • (1) Shipping case for CX100

*custom kits are available, contact MiTeGen with specific requests.


Order Beamline Kits